A microscale approach to organic laboratory techniques / (Record no. 10193)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 07586nam a2200397Ia 4500 |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20260803094214.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 251212s2018 xx 000 0 und d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER | |
| International Standard Book Number | 9781305968349 |
| 050 ## - LIBRARY OF CONGRESS CALL NUMBER | |
| Classification number | 547.007 P28m 2018 |
| 100 ## - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Pavia, Donald L. |
| 245 1# - TITLE STATEMENT | |
| Title | A microscale approach to organic laboratory techniques / |
| Statement of responsibility, etc. | Donald L. Pavia, Gary M. Lampman, George S. Kriz, [and] Randall G. Engel. |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Place of publication, distribution, etc. | Boston, MA : |
| Name of publisher, distributor, etc. | Cengage Learning, |
| Date of publication, distribution, etc. | 2018. |
| 250 ## - EDITION STATEMENT | |
| Edition statement | Sixth edition |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | xvii, 1034 pages: |
| Other physical details | illustrations |
| 300 ## - PHYSICAL DESCRIPTION | |
| Dimensions | 28 cm. |
| 336 ## - CONTENT TYPE | |
| Content type term | text |
| 337 ## - MEDIA TYPE | |
| Media type term | unmediated |
| 338 ## - CARRIER TYPE | |
| Carrier type term | volume |
| 490 ## - SERIES STATEMENT | |
| Series statement | Cengage Learning Laboratory Series for Organic Chemistry |
| 500 ## - GENERAL NOTE | |
| General note | Includes index |
| 546 ## - LANGUAGE NOTE | |
| Language note | in English |
| 505 ## - FORMATTED CONTENTS NOTE | |
| Formatted contents note | Experiment 1.Introduction to Microscale Laboratory.Experiment 2.Solubility.Experiment 3.Crystallization.Experiment 4.Extraction.Experiment 5.A Separation and Purification Scheme.Experiment 6.Chromatography.Experiment 7.Infrared Spectroscopy and Boiling Point Determination.Experiment 8.Simple and Fractional Distillation.Essay: Aspirin.Experiment 9.Acetylsalicylic Acid.Essay: Analgesics.Experiment 10. Isolation of the Active Ingredient in an Analgesic Drug.Experiment 11, Acetaminophen.Essay: Identification of Drugs.Experiment 12. TLC Analysis of Analgesic Drugs.Essay: Caffeine.Experiment 13. Isolation of Caffeine from Tea or Coffee.Essay: Esters -- Flavors and Fragrances.Experiment 14. Isopentyl Acetate (Banana Oil).Essay: Terpenes and Phenylpropanoids.Experiment 15. Essential Oils: Extraction of Oil of Cloves by Steam Distillation.Essay: Stereochemical Theory of Odor.Experiment 16. Spearmint and Caraway Oil: (+)- and (-)-Carvones.Essay: The Chemistry of Vision.Experiment 17. Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Essay: Ethanol and Fermentation Chemistry.Experiment 18. Ethanol from Sucrose.Essay Molecular Modeling and Molecular Mechanics.Experiment 19. An Introduction to Molecular Modeling.Essay: Computational Chemistry -- Ab Initio and Semiempirical Methods.Experiment 20. Computational Chemistry.Experiment 21. Reactivities of Some Alkyl Halides.Experiment 22. Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment 23. Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment 24. 4-Methylcyclohexene.Essay: Fats and Oils.Experiment 25. Methyl Stearate from Methyl Oleate.Essay: Soap.Experiment 26. Preparation of Soap.Essay: Petroleum and Fossil Fuels.Experiment 27. Gas Chromatographic Analysis of Gasolines.Essay: Biofuels.Experiment 28. Biodiesel.Essay: Green Chemistry.Experiment 29. Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination.Experiment 30. Nitration of Aromatic Compounds Using a Recyclable Catalyst.Experiment 31. Reduction of Ketones Using Carrots as Biological Reducing Agents.Experiment 32. Resolution of Phenylethylamine and Determination of Optical Purity.Experiment 33. An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.Experiment 34. Multi-Step Reaction Sequences: The Conversion of Benzaldehydeto Benzilic Acid.Experiment 35. Triphenylmethanol and Benzoic Acid.Experiment 36. Aqueous-based Organozinc Reactions.Experiment 37. Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.Experiment 38. Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.Experiment 39. The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).Experiment 40. A Green Enantioselective Aldol Condensation Reaction.Experiment 41. Preparation of an Unsaturated Ketone via Michael and Aldol Condensation Reactions.Experiment 42. Preparation of Triphenylpyridine.Experiment 43. The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-Butadiene.Experiment 44. Relative Reactivities of Several Aromatic Compounds.Experiment 45. Nitration of Methyl Benzoate.Essay: Synthetic Dyes.Experiment 46. Preparation of Methyl Orange.Experiment 47. Preparation of Indigo.Experiment 48. Formulation of a Paint and Art Project.Essay: Local Anesthetics.Experiment 49. Benzocaine.Essay: Pheromones: Insect Attractants and Repellents.Experiment 50. N,N-Diethyl-m-toluamide: The Insect Repellent OFF".Essay: Sulfa Drugs.Experiment 51. Sulfa Drugs: Preparation of Sulfanilamide.Essay: Polymers and Plastics.Experiment 52. Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.Essay: Diels-Alder Reactions and Insecticides.Experiment 53. The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.Experiment 54. The Diels-Alder Reaction with Anthracene-9-Methanol.Experiment 55. Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone.Essay: Fireflies and Photochemistry.Experiment 56. Luminol.Experiment 57. Identification of Unknowns.Experiment 58. Preparation of a C-4 or C-5 Acetate Ester.Experiment 59. Competing Nucleophiles in SN1 and SN2 Reactions: Investigations Using 2-Pentanol and 3-Pentanol.Experiment 60. Friedel-Crafts Acylation.Experiment 61. The Analysis of Antihistamine Drugs by Gas Chromatography-Mass Spectrometry.Experiment 62. The Use of Organozinc Reagents in Synthesis: An Exercise in Synthesis and Structure Proof by Spectroscopy.Experiment 63. Synthesis of Naproxen by Palladium Catalysis.Experiment 64. The Aldehyde Enigma.Experiment 65. Synthesis of Substituted Chalcones: A Guided-Inquiry Experience.Experiment 66. Green Epoxidation of Chalcones.Experiment 67. Cyclopropanation of Chalcones.Experiment 68. Michael and Aldol Condensation Reactions.Experiment 69. Esterification Reactions of Vanillin: The Use of NMR to Solve a Structure Proof Problem. Technique 1. Laboratory Safety.Technique 2. The Laboratory Notebook, Calculations, and Laboratory Records.Technique 3. Laboratory Glassware: Care and Cleaning.Technique 4. How to Find Data for Compounds: Handbooks and Catalogs.Technique 5. Measurement of Volume and Weight.Technique 6. Heating and Cooling Methods.Technique 7. Reaction Methods.Technique 8. Filtration.Technique 9. Physical Constants of Solids: The Melting Point.Technique 10. Solubility.Technique 11. Crystallization: Purification of Solids.Technique 12. Extractions, Separations, and Drying Agents.Technique 13. Physical Constants of Liquids: The Boiling Point and Density.Technique 14. Simple Distillation.Technique 15. Fractional Distillation, Azeotropes.Technique 16. Vacuum Distillation, Manometers.Technique 17. Sublimation.Technique 18. Steam Distillation.Technique 19. Column Chromatography.Technique 20. Thin-Layer Chromatography.Technique 21. High-Performance Liquid Chromatography (HPLC).Technique 22. Gas Chromatography.Technique 23. Polarimetry.Technique 24. Refractometry.Technique 25. Infrared Spectroscopy.Technique 26. Nuclear Magnetic Resonance Spectroscopy.Technique 27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique 28. Mass Spectrometry.Technique 29. Guide to the Chemical Literature.Appendix 1: Tables of Unknowns and Derivatives.Appendix 2: Procedures for Preparing Derivatives.Appendix 3: Index of Spectra.Index." |
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| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | Organic chemistry |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | CHEMISTRY |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | Chemistry |
| Form subdivision | Laboratory manuals |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | Chemistry |
| General subdivision | Organic |
| Form subdivision | Laboratory manual |
| 700 ## - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Lampman, Gary M.; Kriz, George S.; Engel, Randall G. |
| 944 ## - | |
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| 943 ## - EQUIVALENCE OR CROSS-REFERENCE--COLLECTIVE TITLE [OBSOLETE] [CAN/MARC only] | |
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| Date of treaty signing | 0 |
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| Date of a work | 0 |
| Miscellaneous information | 0 |
| Medium | 1 |
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| 953 ## - | |
| -- | SH0296 |
| 953 ## - | |
| -- | Senior High School Library |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Library of Congress Classification |
| Koha item type | Books |
| Institution code [OBSOLETE] | lisuga |
| -- | 2018-05-28 13:42:50 |
| -- | lisuga |
| Edition | 2018-05-28 13:42:50 |
| 998 ## - LOCAL CONTROL INFORMATION (RLIN) | |
| MyRDA biblio | 10258 |
| Withdrawn status | Lost status | Source of classification or shelving scheme | Damaged status | Not for loan | Home library | Current library | Shelving location | Date acquired | Full call number | Barcode | Date last seen | Price effective from | Koha item type |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Dewey Decimal Classification | FEU - Cavite Basic Education | FEU - Cavite Basic Education | BED Library | 12/21/2025 | CIR 547.007 P28m 2018 | SH0296 | 12/21/2025 | 12/21/2025 | Books |